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Monday, October 3, 2016

SUMMER RESEARCH: SURF


Hello, my name is Emily Conkling and I’m a junior in Environmental and Ecological Engineering. This past summer, I worked with Dr. Andrew Whelton through the Purdue SURF (Summer Undergraduate Research Fellowship) Program.

These are pictures of me during my SURF presentation, and during field work in California.
The project I worked on studied the environmental affects and occupational hazards of working with cured-in-place pipe (or CIPP). CIPP is a method of repairing faulty sewer and storm water pipes. This method involves inverting a resin-impregnated tube into the faulty pipe and curing it in place - basically making a new pipe within the old one. It’s a convenient option because the new pipe can be installed in one day, and it doesn’t involve tearing up asphalt or concrete or cause any long-term road construction.









 The left picture is a piece of rehabilitated pipe. The CIPP is the blue pipe that sits within the old pipe. The right picture shows what the uncured resin looks like before it is cured within a pipe, like in the left picture.







One issue with CIPP is that its chemical composition (and therefore its environmental effects) are very poorly understood. We know that it’s fiberglass reinforced and contains a chemical compound called styrene, but other than that, we don’t know much. Despite this lack of knowledge, this CIPP resin has been assumed to be the cause of downstream fish kills and algal blooms, and adverse health effects in humans. So my team and I set out to find out what exactly was happening with this stuff.


Dr. Whelton and Professor Howarter on site at Purdue

One of the first things we looked at was the resin itself, both cured and uncured. We analyzed these by putting little pieces of it in different solvents, which basically break down and extract whatever chemicals are in the CIPP resin. Once those ‘soaked’ for 14 days, the solvent was put into the GC/MS (Gas Chromatography/Mass Spectrometry). This machine divides up the chemicals and tells you what they are based on molecular weight. This whole process told us some of the chemicals present in CIPP and its resin.
The next step was to figure out what chemicals escaped during the CIPP installation. Luckily for us, there were a few installations scheduled for Purdue’s campus. We took monitoring and sampling equipment with us to the installation. We brought a photoionization detector (or PID) which was calibrated to measure the concentration of styrene in the air. We also brought pumps with sorbent tubes attached, and bag sampling pumps. The sorbent tubes are little metal tubes about 4” long and chemicals in the air sorb, or stick, on to the tube. You can then take this tube back to the lab and analyze it using the GC/MS. Bag sampling pumps are pumps that suck the surrounding air into a tedlar bag, which is a laboratory-grade Ziploc bag. Again, you can analyze the bags of air using the GC/MS.
All of this work was done in preparation for doing field work in California. We wanted to make sure we had a good idea of what to look for before we packed up all the equipment and headed west. In early August, we loaded up a Purdue van, and made the 40 hour trek to Sacramento, California.


We stopped in Laramie, Wyoming the first night. I took this picture before we got back on the interstate in the morning.


We also stopped by the Bonneville Salt Flats in Utah, home of the world land speed records.
Team meeting before field work begins
Have to make sure the respirators fit!
For the most part, we used the same procedure in California as we did at Purdue, just on a larger scale. One main difference was that we took a stainless steel apparatus to California. The purpose of this device was to integrate all of the equipment I talked about before into one big system. Instead of having one machine over here and another machine over there, all of our field equipment was side-by-side. This made things easier for us to operate, and also helped ensure that our data would be comparable.


This is me prepping a PID before we begin our work for the day.

This is our lab in California. As you can see, we pack light.

















Now that we are back in our lab at Purdue, all the analyzing begins. The tedlar bags were analyzed first, followed by the sorbent tubes. Next on the docket is uncured and cured CIPP samples, followed by other things collected on site.
Going into the SURF program, I wasn’t sure what I would think of it. I assumed that I’d be stuck in a lab working on something that wouldn’t really be applicable in the ‘real world.’ And I’m glad that SURF proved me wrong. My work this summer got me outside, doing something different every day, and it’s something that will have direct impacts on the real world. Undergraduate research is definitely something I have grown to really like, and I highly recommend it to other students. It’s a great way to meet other students, get to know faculty, and get some really good experience that will make you valuable to recruiters. After this experience, I am seriously considering getting a Master’s degree, and I’m incredibly thankful for my research team, SURF, and Purdue. Boiler Up!

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